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&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;USP<467> residual solvents-Applying the Agilent 5977A MSD with the Agilent 7697A headspace sampler and Agilent 7890B GC (PDF)

The analysis of Class1, Class 2A, and Class 2B residual solvents are demonstrated at USP 467 limit concentrations using the 5977 MSD with the 7890B and 7697A Headspace sampler

  • Publication Part Number: 5991-2079EN
  • Created: 21 Mar 2013
  • 2 MB
  • PDF
Quick View &#24517;&#23041;&#20307;&#32946;&#36187;&#20107;&#25237;&#27880;Supporting Products Supporting Documents
Publication Part Number 5991-2079EN
Analysis Analysed with Part No.
VF-624ms
Instrument
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 5977
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7697 headspace sampler
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
MMI
Detection
MS
Sample Chemical Group
residual solvents
Sample Matrix
test mixture
Chinese (Simplified) (China) Complete (PDF)
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Applications
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Analysis of USP <467> Residual Solvents using the Agilent 7697A Headspace Sampler with the Agilent 7890B Gas Chromatograph (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;USP residual solvents were analyzed by static headspace on the Agilent 7697A Headspace Sampler combined with the Agilent 7890B Gas Chromatograph.

  • Publication Part Number: 5991-1834EN
  • Created: 29 Jan 2013
  • 340 KB
  • PDF
Quick View &#24517;&#23041;&#20307;&#32946;&#36187;&#20107;&#25237;&#27880;Supporting Products
Publication Part Number 5991-1834EN
Analysis Analysed with Part No.
HP-INNOWax
VF-624ms
Instrument
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7697 headspace sampler
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7890B
Analytical Technique Technique
GC
GC-Capillary
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split/splitless
Detection
FID
Sample Chemical Group
residual solvents
Sample Matrix
test mixture
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Applications
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Analysis of USP <467> Residual Solvents with Improved Repeatability Using the Agilent 7697A Headspace Sampler (PDF)

The 7697A Headspace coupled to a 7890 GC was used for the analysis of UPS Class 1 and Class 2 residual solvents at their USP limit concentrations in aqueous solution.

  • Publication Part Number: 5990-7625EN
  • Created: 22 Aug 2012
  • 1 MB
  • PDF
Quick View &#24517;&#23041;&#20307;&#32946;&#36187;&#20107;&#25237;&#27880;Supporting Products
Publication Part Number 5990-7625EN
Analysis Analysed with Part No.
DB-624
HP-INNOWax
VF-624ms
Instrument
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7697 headspace sampler
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7890
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
split/splitless
Detection
FID
MS
Sample Chemical Group
residual solvents
Sample Matrix
pharmaceuticals
solvent standards
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Applications
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Residual Solvent Analysis with a Specifically Designed and Tested Agilent J&W DB-Select 624UI for USP <467> Column (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Specifically designed and tested Agilent J&W DB-Select 624UI for USP resolves critical pairs.

  • Publication Part Number: 5991-0616EN
  • Created: 07 June 2012
  • 2 MB
  • PDF
Quick View &#24517;&#23041;&#20307;&#32946;&#36187;&#20107;&#25237;&#27880;Supporting Products
Publication Part Number 5991-0616EN
Analysis Analysed with Part No.
DB-Select 624UI for USP 467
Instrument
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 5975C
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7697 headspace sampler
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7890
Analytical Technique Technique
GC
GC/MS
Injection
MMI
Detection
FID
MS
Sample Chemical Group
residual solvents
Sample Matrix
test mixture
Example category image description
Applications
USP 467 Residual Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;For USP-467 with Agilent J&W VF-624ms, replacing a 30 m x 0.32 mm column for one of 15 m x 0.15 mm reduces analysis time by more than half.because the efficiency is higher.

  • Publication Part Number: A02430
  • Created: 11 May 2010
  • 1 MB
  • PDF
Quick View &#24517;&#23041;&#20307;&#32946;&#36187;&#20107;&#25237;&#27880;Supporting Products
Publication Part Number A02430
Analysis Analysed with Part No.
VF-624ms
Instrument
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Analytical Technique Technique
GC
GC-Capillary
Injection
split
Detection
FID
Sample Chemical Group
solvents
Sample Matrix
test mixture

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