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&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Analysis of USP <467> Residual Solvents using the Agilent 7697A Headspace Sampler with the Agilent 7890B Gas Chromatograph (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;USP residual solvents were analyzed by static headspace on the Agilent 7697A Headspace Sampler combined with the Agilent 7890B Gas Chromatograph.

  • Publication Part Number: 5991-1834EN
  • Created: 29 Jan 2013
  • 340 KB
  • PDF
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Publication Part Number 5991-1834EN
Analysis Analysed with Part No.
HP-INNOWax
VF-624ms
Instrument
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7697 headspace sampler
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7890B
Analytical Technique Technique
GC
GC-Capillary
Injection
split/splitless
Detection
FID
Sample Chemical Group
residual solvents
Sample Matrix
test mixture
Chinese (Simplified) (China) Complete (PDF)
Russian (Russia) Complete (PDF)
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Applications
使用安捷倫 7697A 頂空進樣器進行 USP <467> 溶劑殘留的高精度分析 (PDF)

  • Publication Part Number: 5990-7625CHCN
  • Created: 27 Dec 2012
  • 863 KB
  • PDF
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Publication Part Number 5990-7625EN
Analysis Analysed with Part No.
DB-624
HP-INNOWax
VF-624ms
Instrument
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7697 headspace sampler
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7890
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
split/splitless
Detection
FID
MS
Sample Chemical Group
residual solvents
Sample Matrix
pharmaceuticals
solvent standards
English (United States) Complete (PDF)
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Applications
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Residual Solvent Analysis with a Specifically Designed and Tested Agilent J&W DB-Select 624UI for USP <467> Column (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Specifically designed and tested Agilent J&W DB-Select 624UI for USP resolves critical pairs.

  • Publication Part Number: 5991-0616EN
  • Created: 07 June 2012
  • 2 MB
  • PDF
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Publication Part Number 5991-0616EN
Analysis Analysed with Part No.
DB-Select 624UI for USP 467
Instrument
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 5975C
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7697 headspace sampler
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7890
Analytical Technique Technique
GC
GC/MS
Injection
MMI
Detection
FID
MS
Sample Chemical Group
residual solvents
Sample Matrix
test mixture
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;GC analysis of 14 USP 467 solvents on an Agilent J&W VF-200ms column takes 15 minutes.

  • Publication Part Number: A02204
  • Created: 31 Oct 2011
  • 540 KB
  • PDF
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Publication Part Number A02204
Analysis Analysed with Part No.
VF-200ms
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
split
Detection
MS
MS-Ion Trap
Sample Chemical Group
solvents
Sample Matrix
DMSO
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography with headspace analysis and an Agilent J&W CP-Select 624 CB column separates 18 solvent standards in DMSO in 30 minutes.

  • Publication Part Number: A01389
  • Created: 31 Oct 2011
  • 573 KB
  • PDF
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Publication Part Number A01389
Analysis Analysed with Part No.
Select 624 CB
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
Injection
headspace
split
Detection
FID
Sample Chemical Group
solvents
Sample Matrix
standard mixture
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography using an Agilent J&W CP-1301 column separates 26 residual solvents in 49 minutes.

  • Publication Part Number: A01266
  • Created: 31 Oct 2011
  • 808 KB
  • PDF
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Publication Part Number A01266
Analysis Analysed with Part No.
CP-1301
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
Injection
split
Detection
FID
Sample Chemical Group
solvents
Sample Matrix
standard mixture
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography with an Agilent J&W PoraBOND U column separates 32 solvents in 44 minutes, according to USP 467.

  • Publication Part Number: A01546
  • Created: 31 Oct 2011
  • 892 KB
  • PDF
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Publication Part Number A01546
Analysis Analysed with Part No.
PoraBOND U
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
Injection
split
Detection
FID
Sample Chemical Group
solvents
Sample Matrix
DMSO
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography with a 0.15 mm id Agilent J&W CP-Sil 5 CB column separates residual solvents in less than seven minutes.

  • Publication Part Number: A01502
  • Created: 31 Oct 2011
  • 788 KB
  • PDF
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Publication Part Number A01502
Analysis Analysed with Part No.
CP-Sil 5 CB
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
Injection
split
Detection
FID
Sample Chemical Group
residual solvents
solvents
Sample Matrix
pharmaceuticals
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography with a 0.15 mm id Agilent J&W CP-Sil 5 CB column reduces run time in the separation of residual solvents from 25 minutes to less than seven minutes.

  • Publication Part Number: A01501
  • Created: 31 Oct 2011
  • 660 KB
  • PDF
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Publication Part Number A01501
Analysis Analysed with Part No.
CP-Sil 5 CB
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
Injection
split
Detection
FID
Sample Chemical Group
solvents
Sample Matrix
liquids
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography with an Agilent J&W PoraBOND Q column separates 26 solvents in DMSO in 27 minutes.

  • Publication Part Number: A01424
  • Created: 31 Oct 2011
  • 1 MB
  • PDF
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Publication Part Number A01424
Analysis Analysed with Part No.
PoraBOND Q
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
GC-Megabore 0.53 mm ID
Injection
split
Detection
FID
Sample Chemical Group
solvents
Sample Matrix
standard mixture
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography using an Agilent J&W CP-Select 624 CB column separates 26 pharmacopoeia-specified solvents in 30 minutes.

  • Publication Part Number: A01304
  • Created: 31 Oct 2011
  • 845 KB
  • PDF
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Publication Part Number A01304
Analysis Analysed with Part No.
Select 624 CB
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
valve
Detection
MS
Sample Chemical Group
residual solvents
solvents
Sample Matrix
standard mixture
Example category image description
Applications
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Analysis of USP-467 Residual Solvents using Agilent J&W FactorFour VF-WAXms GC Columns (PDF)

Graphical analysis ot residual solvents of USP 467.

  • Publication Part Number: SI-00944
  • Created: 08 Oct 2010
  • 216 KB
  • PDF
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Publication Part Number SI-00944
Analysis Analysed with Part No.
VF-WAXms
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
Injection
split
Detection
FID
Sample Chemical Group
solvents
Sample Matrix
test mixture
Example category image description
Applications
USP 467 Residual Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;For USP-467 with Agilent J&W VF-624ms, replacing a 30 m x 0.32 mm column for one of 15 m x 0.15 mm reduces analysis time by more than half.because the efficiency is higher.

  • Publication Part Number: A02430
  • Created: 11 May 2010
  • 1 MB
  • PDF
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Publication Part Number A02430
Analysis Analysed with Part No.
VF-624ms
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
Injection
split
Detection
FID
Sample Chemical Group
solvents
Sample Matrix
test mixture
Example category image description
Applications
USP-467 residual solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography with an Agilent J&W VF-624ms column separates 27 residual solvents in 40 minutes.

  • Publication Part Number: A02400
  • Created: 11 May 2010
  • 807 KB
  • PDF
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Publication Part Number A02400
Analysis Analysed with Part No.
VF-624ms
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
Injection
split
Detection
FID
Sample Chemical Group
residual solvents
Sample Matrix
test mixture

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