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&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;USP<467> residual solvents-Applying the Agilent 5977A MSD with the Agilent 7697A headspace sampler and Agilent 7890B GC (PDF)

The analysis of Class1, Class 2A, and Class 2B residual solvents are demonstrated at USP 467 limit concentrations using the 5977 MSD with the 7890B and 7697A Headspace sampler

  • Publication Part Number: 5991-2079EN
  • Created: 21 Mar 2013
  • 2 MB
  • PDF
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Publication Part Number 5991-2079EN
Analysis Analysed with Part No.
VF-624ms
Instrument
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 5977
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7697 headspace sampler
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
MMI
Detection
MS
Sample Chemical Group
residual solvents
Sample Matrix
test mixture
Chinese (Simplified) (China) Complete (PDF)
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Applications
使用安捷倫 7697A 頂空進樣器進行 USP <467> 溶劑殘留的高精度分析 (PDF)

  • Publication Part Number: 5990-7625CHCN
  • Created: 27 Dec 2012
  • 863 KB
  • PDF
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Publication Part Number 5990-7625EN
Analysis Analysed with Part No.
DB-624
HP-INNOWax
VF-624ms
Instrument
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7697 headspace sampler
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7890
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
split/splitless
Detection
FID
MS
Sample Chemical Group
residual solvents
Sample Matrix
pharmaceuticals
solvent standards
English (United States) Complete (PDF)
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Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography using an Agilent J&W CP-Select 624 CB column separates 26 pharmacopoeia-specified solvents in 30 minutes.

  • Publication Part Number: A01304
  • Created: 31 Oct 2011
  • 845 KB
  • PDF
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Publication Part Number A01304
Analysis Analysed with Part No.
Select 624 CB
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
valve
Detection
MS
Sample Chemical Group
residual solvents
solvents
Sample Matrix
standard mixture
Example category image description
Applications
Hydroxy-alprazolam in urine (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Using Agilent SPEC DAU for sample prep, and an Agilent J&W VF-DA, it was possible to determine hydroxy-alprazolam in Full Scan with confirmation by library search.

  • Publication Part Number: A01982
  • Created: 31 Oct 2011
  • 1 MB
  • PDF
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Publication Part Number A01982
Analysis Analysed with Part No.
VF-DA
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
splitless
Detection
MS
Sample Chemical Group
drug screens
drugs
Sample Matrix
urine
Example category image description
Applications
Allergens (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Analyze allergens in 400 seconds by GC using a 0.1 mm id Agilent J&W VF-5ms column.

  • Publication Part Number: A02220
  • Created: 31 Oct 2011
  • 2 MB
  • PDF
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Publication Part Number A02220
Analysis Analysed with Part No.
VF-5ms
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
splitless
Detection
MS
Sample Chemical Group
allergens
Sample Matrix
test mixture
Example category image description
Applications
Halogenated hydrocarbons (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography with an Agilent J&W PoraPLOT Q column separates four anesthetic gases in 18 minutes.

  • Publication Part Number: A01627
  • Created: 31 Oct 2011
  • 403 KB
  • PDF
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Publication Part Number A01627
Analysis Analysed with Part No.
PoraPLOT Q
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
headspace
Detection
MS
Sample Chemical Group
anaesthetics
halogenated hydrocarbons
Sample Matrix
air
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;GC analysis of 14 USP 467 solvents on an Agilent J&W VF-200ms column takes 15 minutes.

  • Publication Part Number: A02204
  • Created: 31 Oct 2011
  • 540 KB
  • PDF
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Publication Part Number A02204
Analysis Analysed with Part No.
VF-200ms
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
split
Detection
MS
MS-Ion Trap
Sample Chemical Group
solvents
Sample Matrix
DMSO
Example category image description
Applications
Cholestanyl derivatives (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;GC/MS with an Agilent J&W VF-Xms column delivers symmetrical peaks with virtually no bleed in the analysis of cholestanyl derivatives.

  • Publication Part Number: A01963
  • Created: 31 Oct 2011
  • 1 MB
  • PDF
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Publication Part Number A01963
Analysis Analysed with Part No.
VF-Xms
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
splitless
Detection
MS
Sample Chemical Group
cholestanyl derivatives
Sample Matrix
solvent
Example category image description
Applications
Sugars (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Separation of 21 TMS-derivatized sugars using gas chromatography and Agilent J&W VF-1ms in 36 minutes.

  • Publication Part Number: A02337
  • Created: 11 May 2010
  • 651 KB
  • PDF
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Publication Part Number A02337
Analysis Analysed with Part No.
VF-1ms
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
split
Detection
MS
Sample Chemical Group
carbohydrates
sugars
Sample Matrix
test mixture
Example category image description
Applications
Steroids as HFBA esters (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Determination of eight steroids in urine on Agilent J&W VF-17ms in less than 22 minutes.

  • Publication Part Number: A02389
  • Created: 11 May 2010
  • 586 KB
  • PDF
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Publication Part Number A02389
Analysis Analysed with Part No.
VF-17ms
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
splitless
Detection
MS
Sample Chemical Group
steroids
Sample Matrix
urine
Example category image description
Applications
Steroids as HFBA esters (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent J&W VF-17ms separates interference and methylandrostandiol in urine steroids analysis, but deconvolution via MS is not possible because of similar mass.

  • Publication Part Number: A02390
  • Created: 11 May 2010
  • 703 KB
  • PDF
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Publication Part Number A02390
Analysis Analysed with Part No.
VF-17ms
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
splitless
Detection
MS
Sample Chemical Group
steroids
Sample Matrix
urine

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