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&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;USP<467> residual solvents-Applying the Agilent 5977A MSD with the Agilent 7697A headspace sampler and Agilent 7890B GC (PDF)

The analysis of Class1, Class 2A, and Class 2B residual solvents are demonstrated at USP 467 limit concentrations using the 5977 MSD with the 7890B and 7697A Headspace sampler

  • Publication Part Number: 5991-2079EN
  • Created: 21 Mar 2013
  • 2 MB
  • PDF
Quick View &#24517;&#23041;&#20307;&#32946;&#36187;&#20107;&#25237;&#27880;Supporting Products Supporting Documents
Publication Part Number 5991-2079EN
Analysis Analysed with Part No.
VF-624ms
Instrument
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 5977
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7697 headspace sampler
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
MMI
Detection
MS
Sample Chemical Group
residual solvents
Sample Matrix
test mixture
Chinese (Simplified) (China) Complete (PDF)
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Applications
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Analysis of USP <467> Residual Solvents using the Agilent 7697A Headspace Sampler with the Agilent 7890B Gas Chromatograph (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;USP residual solvents were analyzed by static headspace on the Agilent 7697A Headspace Sampler combined with the Agilent 7890B Gas Chromatograph.

  • Publication Part Number: 5991-1834EN
  • Created: 29 Jan 2013
  • 340 KB
  • PDF
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Publication Part Number 5991-1834EN
Analysis Analysed with Part No.
HP-INNOWax
VF-624ms
Instrument
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7697 headspace sampler
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7890B
Analytical Technique Technique
GC
GC-Capillary
Injection
split/splitless
Detection
FID
Sample Chemical Group
residual solvents
Sample Matrix
test mixture
Russian (Russia) Complete (PDF)
Chinese (Simplified) (China) Complete (PDF)
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Applications
使用安捷倫 7697A 頂空進樣器進行 USP <467> 溶劑殘留的高精度分析 (PDF)

  • Publication Part Number: 5990-7625CHCN
  • Created: 27 Dec 2012
  • 863 KB
  • PDF
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Publication Part Number 5990-7625EN
Analysis Analysed with Part No.
DB-624
HP-INNOWax
VF-624ms
Instrument
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7697 headspace sampler
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7890
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
split/splitless
Detection
FID
MS
Sample Chemical Group
residual solvents
Sample Matrix
pharmaceuticals
solvent standards
English (United States) Complete (PDF)
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Applications
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Residual Solvent Analysis with a Specifically Designed and Tested Agilent J&W DB-Select 624UI for USP <467> Column (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Specifically designed and tested Agilent J&W DB-Select 624UI for USP resolves critical pairs.

  • Publication Part Number: 5991-0616EN
  • Created: 07 June 2012
  • 2 MB
  • PDF
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Publication Part Number 5991-0616EN
Analysis Analysed with Part No.
DB-Select 624UI for USP 467
Instrument
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 5975C
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7697 headspace sampler
&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Agilent 7890
Analytical Technique Technique
GC
GC/MS
Injection
MMI
Detection
FID
MS
Sample Chemical Group
residual solvents
Sample Matrix
test mixture
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography using an Agilent J&W CP-Select 624 CB column separates 26 pharmacopoeia-specified solvents in 30 minutes.

  • Publication Part Number: A01304
  • Created: 31 Oct 2011
  • 845 KB
  • PDF
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Publication Part Number A01304
Analysis Analysed with Part No.
Select 624 CB
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
valve
Detection
MS
Sample Chemical Group
residual solvents
solvents
Sample Matrix
standard mixture
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography with an Agilent J&W PoraBOND U column separates 32 solvents in 44 minutes, according to USP 467.

  • Publication Part Number: A01546
  • Created: 31 Oct 2011
  • 892 KB
  • PDF
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Publication Part Number A01546
Analysis Analysed with Part No.
PoraBOND U
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
Injection
split
Detection
FID
Sample Chemical Group
solvents
Sample Matrix
DMSO
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography with headspace analysis and an Agilent J&W CP-Select 624 CB column separates 18 solvent standards in DMSO in 30 minutes.

  • Publication Part Number: A01389
  • Created: 31 Oct 2011
  • 573 KB
  • PDF
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Publication Part Number A01389
Analysis Analysed with Part No.
Select 624 CB
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
Injection
headspace
split
Detection
FID
Sample Chemical Group
solvents
Sample Matrix
standard mixture
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography with a 0.15 mm id Agilent J&W CP-Sil 5 CB column reduces run time in the separation of residual solvents from 25 minutes to less than seven minutes.

  • Publication Part Number: A01501
  • Created: 31 Oct 2011
  • 660 KB
  • PDF
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Publication Part Number A01501
Analysis Analysed with Part No.
CP-Sil 5 CB
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
Injection
split
Detection
FID
Sample Chemical Group
solvents
Sample Matrix
liquids
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography using an Agilent J&W CP-1301 column separates 26 residual solvents in 49 minutes.

  • Publication Part Number: A01266
  • Created: 31 Oct 2011
  • 808 KB
  • PDF
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Publication Part Number A01266
Analysis Analysed with Part No.
CP-1301
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
Injection
split
Detection
FID
Sample Chemical Group
solvents
Sample Matrix
standard mixture
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography with a 0.15 mm id Agilent J&W CP-Sil 5 CB column separates residual solvents in less than seven minutes.

  • Publication Part Number: A01502
  • Created: 31 Oct 2011
  • 788 KB
  • PDF
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Publication Part Number A01502
Analysis Analysed with Part No.
CP-Sil 5 CB
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
Injection
split
Detection
FID
Sample Chemical Group
residual solvents
solvents
Sample Matrix
pharmaceuticals
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;GC analysis of 14 USP 467 solvents on an Agilent J&W VF-200ms column takes 15 minutes.

  • Publication Part Number: A02204
  • Created: 31 Oct 2011
  • 540 KB
  • PDF
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Publication Part Number A02204
Analysis Analysed with Part No.
VF-200ms
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
GC/MS
Injection
split
Detection
MS
MS-Ion Trap
Sample Chemical Group
solvents
Sample Matrix
DMSO
Example category image description
Applications
Solvents (PDF)

&#24517;&#23041;&#20307;&#32946;&#30331;&#24405;&#25163;&#26426;Gas chromatography with an Agilent J&W PoraBOND Q column separates 26 solvents in DMSO in 27 minutes.

  • Publication Part Number: A01424
  • Created: 31 Oct 2011
  • 1 MB
  • PDF
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Publication Part Number A01424
Analysis Analysed with Part No.
PoraBOND Q
Instrument
---
Analytical Technique Technique
GC
GC-Capillary
GC-Megabore 0.53 mm ID
Injection
split
Detection
FID
Sample Chemical Group
solvents
Sample Matrix
standard mixture

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